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71.
在碱性介质中,痕量Ag(Ⅰ)对新试剂6-(2-羟基-4-二乙基氨苯偶氮)-2,3-二氢-1,4-酞嗪二酮(简称HDEA)的电化学发光具有显著的催化作用。基于此,提出了HDEA-KCI-KOH体系测定矿样中痕量Ag的新方法。方法的检测限为2.0×10~(-8)mol/L Ag,线性范围为5.0×10~(-8)—3.0×10~(-6)mol/L Ag。采用巯基棉富集分离,应用本法测定一些矿样中的Ag,结果良好。 相似文献
72.
At 21:45 hr (Beijing time) on Oct. 31, 1990 the Yanzhuang meteorite hit the ground at the Yanzhuang village, Wenyuan County,
Guangdong Province. Several fragments, totalling 3.5 kg, were recovered during the field survey. This meteorite is a rare
one of its kind due to its heavily shocked features and thick veins made up of black molten materials.
Olivine and low-calcium pyroxene are compositionally homogeneous with Fa=18.59, Fs=16.35 and Wo=1.29. The chemical composition
(total Fe=28.0%) and recrystallized texture of the chondritic mass show that the Yanzhuang is an H6 chondrite. The black molten
materials occur in the form of blocks (up to 2×3×4 cm in size) and veins (0.1–15 mm in width), and contain a lot of rounded
and elliptic FeNi-FeS blobs (up to 6–10 mm in length). The metal in these blobs exhibits distinct dendritic structure characteristic
of rapid cooling. Unmolten and molten samples are very similar in chemical composition, fitting well with the average H-chondrites.
Partial melting and FeNi/FeS-silicate separation have not been observed in the molten materials of the Yanzhuang.
This project was financially supported by the Science Foundation of Guangdong Province. 相似文献
73.
信号内插与噪音剔除是相互有着有机联系的两个方面。首先讨论地震信号的内插方法,提出了一种“最佳内插算子”,从而导出了另一种“检噪算子”,它可以有效地把干扰波从记录中识别出来,并将其“剔除”出去。进而讨论空间域数据的内插问题--道内插问题。在一定的条件下,空间域数据内插与时间域内插是完全等效的,因此道内插也可以采用与时间域相同的“最佳内插算子”。地震记录上的干扰波其绝大部分表现为空间域的脉冲式干扰,所以用“检噪算子”在空间域作褶积,便能识别干扰,从而对干扰加以剔除。本文解决了一种迭代的剔除方法,取得了好的效果。 相似文献
74.
Aromatic hydrocarbons from benzene extracts of New Albany Shale were characterized. A biomarker that has a molecular weight of 546 and a structural configuration consistent with that of an alkyl-aromatic hydrocarbon (C40H66) was tentatively identified. It was found that the relative concentrations of the biomarker are indicative of differing levels of thermal maturity of the shale organic matter. A 40-carbon bicyclic carotenoid (C40H48) is proposed as the geochemical precursor of this biomarker. Thermal maturity of the shale organic matter can also be differentiated by observing differences in “fingerprints” as obtained by field-ionization mass spectrometry on the aromatic hydrocarbon fraction. Using this technique, we found that the more mature shale samples from southeastern Illinois contain more low molecular weight extractable aromatic hydrocarbons and the less mature shale samples from northwestern Illinois contain more high molecular weight extractable aromatic hydrocarbons. It was demonstrated that field-ionization and tandem mass spectrometric techniques through fingerprint and individual compound identification, are useful for shale aromatic hydrocarbon fraction characterization and for thermal maturation interpretation. 相似文献
75.
海底X射线荧光探测系统的软件研制 总被引:2,自引:2,他引:0
基于Windows98操作平台,结合软件工程的设计原则和面向对象的程序设计方法,用Visual Basic 6.0开发了海底X射线荧光探测系统软件(EDXRF^MS)。该软件能完成数据处理及运算,主要解决谱数据的采集与测量控制、成图和图形处理、X射线荧光谱分析、干扰因素的校正、仪器标定与含量计算等问题。EDXRF^MS软件与海底X射线荧光探测系统的硬件配合,能够进行海上现场多道数据的实时采集,对于海底矿产资源的开发具有一定的实用价值。 相似文献
76.
77.
78.
High-resolution climate variability of southwest China during 57-70 ka reflected in a stalagmite δ18O record from Xinya Cave 总被引:1,自引:0,他引:1
Li TingYong Yuan DaoXian Li HongChun Yang Yan Wang JianLi Wang XinYa Li JunYun Qin JiaMing Zhang MeiLiang Lin YuShi 《中国科学D辑(英文版)》2007,50(8):1202-1208
A 26-cm-long stalagmite (XY2) from Xinya Cave in northeastern Chongqing of China has been ICP-MS 230Th/U dated, showing a depositional hiatus at 2.3 cm depth from the top. The growth of the 2.3–26 cm interval determined by
four dates was between 57 ka and 70 ka, with a linear growth rate of 0.023 mm/a. We have analyzed 190 samples for δ
18O and δ
13C, mostly in the 2.3–26 cm part. The δ
18O and δ
13C values between 57 ka and 70 ka reveal decadal-to-centennial climatic variability during the glacial interval of Marine Isotope
Stage 4 (MIS4), exhibiting much higher resolution than that of the published Hulu and Dongge records during this interval.
Speleothem δ
18O in eastern China, including our study area can be used as a proxy of summer monsoon strength, with lighter values pointing
to stronger summer monsoon and higher precipitation, and vice versa. Two decreases in the δ
18O signature of XY2 record around 59.5 and 64.5 Ka are argued to correspond to the Dansgaard-Oeschger (D-O) events 17 and 18
respectively. The Heinrich event 6 (H6) can be identified in the record as a heavy δ
18O peak around 60 ka, indicating significant weakening of the monsoon in Chongqing during the cold period. The XY2 δ
18O record shows very rapid change toward to the interstadial condition of the D-O event, but more gradual change toward to
the cold stadial condition. This phenomenon found in the Greenland ice core records is rarely observed so clearly in previously
published speleothem records. According to SPECMAP δ
18O record, the glacial maximum of MIS 4 was around 64.5 ka with the boundary of MIS 3/4 around 60 ka. Unlike the marine record,
the speleothem record of XY2, China, exhibits much high frequency variations without an apparent glacial maximum during MIS
4. However, the timing of MIS 3/4 boundary seems to be around 60 ka when the H6 terminated, in agreement with the marine chronology.
The growth period of sample XY2 during glacial times probably reflects a local karstic routing of water, rather than having
climatic significance.
Supported by the National Natural Science Foundation of China (Grant Nos. 40672165, 90511004, 40672202) and the Academician
Special Project of Chongqing Science Committee (Grant No. 2003-7835) 相似文献
79.
改进了游离二氧化硅(fSiO2)测定中试样的分解方法,采用硫-磷混酸替代单独使用磷酸分解试样,防止了焦磷酸盐的形成,同时,氟硼酸对fSiO2的溶解率符合测定要求。改进的方法用于标准物质中fSiO2的测定,结果与标准值或磷酸溶矿重量法相符。对于ω(fSiO2)=3.26%的标样10次测定的RSD为2.4%。 相似文献
80.
介绍了新水溶性显色剂 2 - ( 2 ,3,5 -三氮唑偶氮 ) - 1 ,8-二羟基 - 3,6-萘二磺酸与钴的显色反应及应用 ,建立了测定钴的新方法。在 pH 9.9的Na2 B4O7 NaOH缓冲液中该试剂与钴形成 1∶1蓝色稳定络合物 ,λmax为 5 88.8nm ,Co的质量浓度在 0~ 1 .0mg/L内符合比尔定律 ,表观摩尔吸光系数为 3.46× 1 0 4 L·mol- 1 ·cm- 1 。所拟方法用于环境水样及维生素B1 2 注射液中的微量钴测定 ,结果与原子吸收法相符 ,5次测定的RSD <1 %。 相似文献